The Reflux Condenser Module is placed on top of the xelsius reactor unit cooling the upper section of reaction vessels, here recondensation of solvent vapor takes place.

The Reflux Condenser Module is integrated into the extant cooling circuit via leak-free quick couplings, making the installation fast and easy.

The design supersedes the need for multiple protruding and fragile glass reflux condensers.

Specifications

Dimension (L x W x H): 352 x 156 x 48 mm

Materials: Casing HDPE, Heat sink sleeves SS

Compatible vessel: Ø = 24 mm, H > 115 mm

For storage of reactor vessels during sample preparation or subsequent work steps following the synthesis the Vial Rack offers 10 positions aside the xelsius reactor.

Two lab stand support rods in the back of the reactor allow the installation of additional components, e.g. nevoLINK boxes (control units).

Specifications

Dimension (L x W x H): 480 x 249 x 94 mm

Material: PTFE coated stainless steel

The On Top Adapter plate is designed to setup the xelsius reactor unit stacked above its power supply unit, thereby the footprint in the laboratory fume hood is halved offering 10 reactor positions at a space requirement of 44.0 x 21.5 cm.

Spilled liquids are collected in a gutter protecting the lower module from exposition to chemicals.

Specifications

Dimension (L x W x H): 440 x 215 x 20 mm

Material: HDPE

For monitoring of the reaction temperature external resistance temperature sensors are connected to the xelsius reactor, this flexible probes are coated with FEP offering high chemical resistance.

Employing this sensors allows the presice regulation of the reaction mediums temperature via the xelsius reactors PI controller. Utilizing fittings and ferrules provides a gas-tight integration of these sensors into the experimental setup.

The temperature sensor is compatible with the 5-port cap.

Specifications

Sensor type: PT1000

Connector: Lemo 5-pole

Measuring range: -30 °C – 170 °C

Accuracy at 100 °C:  ±0.8 °C

Wetted material: FEP

The Dosing Pump Unit is a dual-channel pump system for automated dosing, featuring

• Valveless, high precision micro dosing pump
• Single-shot mode: dispense volume 10 µL to 25 mL per stroke
• Continuous mode: flow rate 20 µL/min to 4 mL/min
• Dosing accuracy: ± 1% of delivered volume
• Integrated calibration function
• Manual control on a front touch pad
• Seamless integration of pump operation into xelsius control software
  Automated dosing in the scope of programmable reaction profile
• High chemical resistance, wetted materials: Al₂O₃ & PVDF

With the Inerting Station 10 reaction vessels can be evacuated  and flushed with inert gas in parallel in a efficient,  reproducible manner.